Benzoylacetone → 2-Methyl-1-phenylbutane-1,3-dione

HRID 132725

Reaction equation

[C:1]([CH2:9][C:10](=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)(=[O:8])[C:2]1C=CC=CC=1.[C:18]1(C(=O)CC(=O)C)C=CC=CC=1>>[C:11]1([C:10](=[O:17])[CH:9]([CH3:18])[C:1](=[O:8])[CH3:2])[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1

Participants

Reactant 2

HCID 7166Benzoylacetone

HCID 8433Dibenzoylmethane

Product 1

HCID 5693692-Methyl-1-phenylbutane-1,3-dione

Procedure

Synthetic procedure was identical with that described in synthetic example 42(1), except that raw material dibenzoyl methane was replaced by 1-phenyl-1,3-butandione.

Sources & evidence

ORD record: ord-721a9390796545f0b4314d4434635ff6
Source dataset: uspto-grants-2008_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07388061B2

Linked notes

Loading…