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2-Butanone oxime → 2-Butoxyethanol

HRID 1362771
Notes
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Reaction equation

HRID 1362771 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][O:5][CH2:6][CH2:7][OH:8].C[C:10](=[N:13]O)CC>>[CH3:1][CH2:2][CH2:3][CH2:4][O:5][CH2:6][CH2:7][OH:8].[N-:13]=[C:10]=[O:5]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 72922-Butanone oximeHCID 81332-Butoxyethanol

Product 2

HCID 81332-ButoxyethanolHCID 105034Isocyanate

Procedure

To the reactant, butyl cellosolve (72.7 parts by mass) was added. Subsequently, the temperature of the reactant was set to 50° C. To the reactant, 25.8 parts by mass of 2-butanone oxime (manufactured by Ardrich) was added dropwise to obtain a butyl cellosolve solution of isocyanate compound D having an average number of functional groups: 3.5.

Workup

  1. customwas set to 50° C

Sources & evidence

ORD record
ord-f12c36f844d1480aa8b8b10df0f3f285
Source dataset
uspto-grants-2011_02
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07881646B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes