2-Butanone oxime → 2-Butoxyethanol

HRID 1362772

Reaction equation

HRID 1362772 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][O:5][CH2:6][CH2:7][OH:8].C[C:10](=[N:13]O)CC>>[CH3:1][CH2:2][CH2:3][CH2:4][O:5][CH2:6][CH2:7][OH:8].[N-:13]=[C:10]=[O:5]

Participants

4

Reactant 2

HCID 72922-Butanone oximeHCID 81332-Butoxyethanol

Product 2

HCID 81332-ButoxyethanolHCID 105034Isocyanate

Procedure

To the reactant, butyl cellosolve (72.7 parts by mass) was added. Subsequently, the temperature of the reactant was set to 50° C. To the reactant, 5.8 parts by mass of 2-butanone oxime (manufactured by Ardrich) was added dropwise to obtain a butyl cellosolve solution of isocyanate compound E having an average number of functional groups: 3.5.

Workup

  1. customwas set to 50° C

Sources & evidence

ORD record
ord-ab3021447c3242d5b06ae0456a103d2e
Source dataset
uspto-grants-2011_02
Patent number
US07881646B2

Linked notes

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