HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Fluoro-1H-indole → 3-(1-Ethyl-5-fluoro-indan-1-yl)-7-fluoro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Fluoro-1H-indole | HCID 2774504 | — |
| Reactant | 1-Ethyl-5-fluoroindan-1-ol | HCID 59340428 | — |
| Product | 3-(1-Ethyl-5-fluoro-indan-1-yl)-7-fluoro-1H-indole | HCID 11565621 | — |
Reaction Steps
Utilizing 1-ethyl-5-fluoro-indan-1-ol and 7-fluoroindole, the title compound is prepared as in example 1. 217 mg (92%). NMR (400 MHz, CDCl3): δ 0.85 (t, 3H), 2.12 (m, 1H), 2.21 (m, 1H), 2.31 (m, 1H), 2.58 (m, 1H), 2.97 (m, 2H), 6.83 (m, 4H), 6.98 (m, 3H), 8.06 (s, 1H, NH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728150B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-b888e303295143afa63cc5b1e99b8fb2 |
| Source note | uspto-grants-2010_06 |