HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-3-isocyanato- → N-(3-Chlorophenyl)-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | N-(3-Chlorophenyl)-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea | HCID 10274205 | — |
Reaction Steps
Example 13 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 1-chloro-3-isocyanatobenzene (16.6 μl) to give the title compound (0.0247 g). LC-MS (System A): Rt 2.46 mins, Mass Spectrum m/z 428 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-ee37355fc4f6429eb130bd652cdc9f51 |
| Source note | uspto-grants-2007_01 |