4-tert-Butyl hydrogen N-((phenylmethoxy)carbonyl)-L-aspartate → HCID 70050186, compound

HRID 1376682

Reaction equation

HRID 1376682 reaction equation
[NH:1]([C:14]([O:16][CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[O:15])[C@H:2]([C:11]([OH:13])=O)[CH2:3][C:4](=[O:10])[O:5][C:6]([CH3:9])([CH3:8])[CH3:7].[NH2:24][C@H:25]([C:29]([O:31][C:32]([CH3:35])([CH3:34])[CH3:33])=[O:30])[CH:26]([CH3:28])[CH3:27]>CCCCCC>[NH:1]([C:14]([O:16][CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[O:15])[C@H:2]([C:11]([NH:24][C@H:25]([C:29]([O:31][C:32]([CH3:34])([CH3:33])[CH3:35])=[O:30])[CH:26]([CH3:28])[CH3:27])=[O:13])[CH2:3][C:4](=[O:10])[O:5][C:6]([CH3:7])([CH3:8])[CH3:9]

Participants

4

Reactant 2

HCID 1110824-tert-Butyl hydrogen N-((phenylmethoxy)carbonyl)-L-aspartateHCID 114626tert-Butyl valinate

Product 1

HCID 70050186HCID 70050186, compoundYield 93%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

By condensing Z-Asp(OtBu)-OH and H-Val-OtBu there is obtained Z-Asp(OtBu)-Val-OtBu, m.p. 75° C. (n-hexane), yield: 93%.

Sources & evidence

ORD record
ord-9c1a31d54e9841e09e768750a489ded0
Source dataset
uspto-grants-1997_09
Patent number
US05663297

Linked notes

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