n-Propylimidazole → HCID 178456359, compound

HRID 1380358

Reaction equation

HRID 1380358 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11]Cl)=[CH:4][CH:3]=1.[CH2:13]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH2:14][CH3:15]>>[Cl-:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N+:18]2[CH:19]=[CH:20][N:16]([CH2:13][CH2:14][CH3:15])[CH:17]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 118785n-PropylimidazoleHCID 200827321-Chloro-4-(4-chlorobutyl)benzene

Product 1

HCID 178456359HCID 178456359, compound

Conditions

Temperature
130 °C

Procedure

Add 7.13 g (0.035 mole) of 1-chloro-4-(4-chlorobutyl)benzene to 3.52 g (0.032 mole) of 1-propyl-1H-imidazole and heat to 130° C. for 18 hours. Follow the progress of reaction by NMR (CDCl3). At the completion of the reaction, cool to room temperature to obtain the title compound.

Workup

  1. customthe progress of reaction by NMR (CDCl3)
  2. customAt the completion of the reaction
  3. temperaturecool to room temperature

Sources & evidence

ORD record
ord-03e1c0abbfd6420db3bce14e5300b696
Source dataset
uspto-grants-1986_04
Patent number
US04581370

Linked notes

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