N-tert-butylhydroxylamine → N-tert-Butyl-alpha-(4-aminosulfonylphenyl)nitrone

HRID 1384384

Reaction equation

[NH2:1][S:2]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])=[O:3].[C:13]([NH:17][OH:18])([CH3:16])([CH3:15])[CH3:14]>>[C:13]([N+:17]([O-:18])=[CH:9][C:8]1[CH:11]=[CH:12][C:5]([S:2]([NH2:1])(=[O:4])=[O:3])=[CH:6][CH:7]=1)([CH3:16])([CH3:15])[CH3:14]

Participants

Reactant 2

HCID 98586N-tert-butylhydroxylamine

HCID 1510884-Sulfamoylbenzaldehyde

Product 1

HCID 73752976N-tert-Butyl-alpha-(4-aminosulfonylphenyl)nitrone

Procedure

Using 4-aminosulfonylbenzaldehyde and N-tert-butylhydroxylamine and following the procedures described herein, the title compound was prepared as a white powder, m.p. 219.1-219.4° C.

Sources & evidence

ORD record: ord-d0b9f29bdb38453ea4c590ff37d928d0
Source dataset: uspto-grants-2001_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06258852B1

Linked notes

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