Methyl 6-Bromohexanoate → 6-[[3-[(3,4-Dimethylphenyl)amino]-4,6-dinitrophenyl]oxy]hexanoic acid methyl ester
Reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([NH:9][C:10]2[CH:11]=[C:12]([OH:22])[C:13]([N+:19]([O-:21])=[O:20])=[CH:14][C:15]=2[N+:16]([O-:18])=[O:17])[CH:5]=[CH:6][C:7]=1[CH3:8].[CH3:23][O:24][C:25](=[O:32])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30]Br>>[CH3:23][O:24][C:25](=[O:32])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][O:22][C:12]1[C:13]([N+:19]([O-:21])=[O:20])=[CH:14][C:15]([N+:16]([O-:18])=[O:17])=[C:10]([NH:9][C:4]2[CH:5]=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[CH:3]=2)[CH:11]=1Participants
3
Procedure
5 g of 3-[(3,4-dimethylphenyl)amino]-4,6-dinitrophenol was O-alkylated with 6-bromohexanoic acid methyl ester at 70° C. analogously to general operating instructions 8.
Sources & evidence
- ORD record
- ord-32139ccb14504c8a89365f00ab6b1103
- Source dataset
- uspto-grants-2008_03