Phenylacetylene → HCID 53247568, compound

Reaction equation

[C:1]([C:5]1[N:14]=[C:8]2[CH:9]=[CH:10][C:11](I)=[CH:12][N:7]2[N:6]=1)([CH3:4])([CH3:3])[CH3:2].[C:15]1([C:21]#[CH:22])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:1]([C:5]1[N:14]=[C:8]2[CH:9]=[CH:10][C:11]([C:22]#[C:21][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[CH:12][N:7]2[N:6]=1)([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 10821Phenylacetylene

HCID 58316712HCID 58316712, compound

Product 1

HCID 53247568HCID 53247568, compound

Procedure

The title compound, a yellow solid, MS: m/e=276.2 (M+H+), can be prepared in accordance with the general method of example 1 from 2-tert-butyl-6-iodo-[1,2,4]triazolo[1,5-a]pyridine (example 39, step 4) and phenylacetylene.

Sources & evidence

ORD record: ord-32c693ea51264e818096677aa82d614f
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08933094B2

Reaction notes

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