Benzene → 19847-64-4
Reaction equation
[CH:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:7](Cl)(=[O:12])/[C:8](=[CH:10]/[CH3:11])/[CH3:9].[Cl-].[Al+3].[Cl-].[Cl-]>ClCCl>[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:12])/[C:8](=[CH:10]/[CH3:11])/[CH3:9]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
Benzene (1 mL), tigloyl chloride (236 mg), and aluminium chloride (160 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (126 mg).
Workup
- additionThe resultant was treated in the same manner
Sources & evidence
- ORD record
- ord-6b8e1fc032b74c878ed095b493b5e8bc
- Source dataset
- uspto-grants-2015_01
- Patent number
- US08937091B2
Reaction notes
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