Phenylhydrazine hydrochloride → 2-Acetylselenophene phenylhydrazone

Reaction equation

Cl.[C:2]1([NH:8][NH2:9])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]([C:13]1[Se:14][CH:15]=[CH:16][CH:17]=1)(=O)[CH3:11]>>[C:2]1([NH:8][N:9]=[C:10]([C:13]2[Se:14][CH:15]=[CH:16][CH:17]=2)[CH3:11])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 60962Phenylhydrazine hydrochloride

HCID 139932Ethanone, 1-selenophene-2-yl-

Product 1

HCID 867521872-Acetylselenophene phenylhydrazone

Procedure

This compound is prepared from commercial phenylhydrazine hydrochloride (Aldrich) and 2-acetylselenophene, which is itself obtained according to the procedure described by S. Umezawa (reference 18).

Workup

customobtained

Sources & evidence

ORD record: ord-b1c4c35e4d754049b51187394fb98649
Source dataset: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05726063

Reaction notes

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