HCID 12428590, compound → HCID 178444824, compound

Reaction equation

[CH3:1][C:2]([N:7]=[C:8]=[N:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)([CH3:6])[CH2:3][CH2:4][CH3:5].C([N:20]=[C:21]=[N:22]C1C=NC=CC=1)(C)(C)C>>[C:21]([N:22]=[C:8]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)[NH:7][C:2]([CH3:1])([CH3:6])[CH2:3][CH2:4][CH3:5])#[N:20]

Participants

Reactant 2

HCID 12428590HCID 12428590, compound

HCID 20501940HCID 20501940, compound

Product 1

HCID 178444824HCID 178444824, compound

Procedure

By following the procedure of Example 1, but substituting N-(1,1-dimethylbutyl)-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the N"-cyano-N-(1,1-dimethylbutyl)-N'-3-pyridylguanidine was obtained with a melting point of 188.0°-188.5° C.

Sources & evidence

ORD record: ord-1373210e61854d33a4bf10a24361c741
Source dataset: uspto-grants-1977_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04057636

Reaction notes

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