HCID 12428590, compound → HCID 178449188, compound

Reaction equation

[CH:1]([N:5]=[C:6]=[N:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)([CH2:3][CH3:4])[CH3:2].C([N:18]=[C:19]=[N:20]C1C=NC=CC=1)(C)(C)C>>[CH:1]([NH:5][C:6]([NH:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)=[N:20][C:19]#[N:18])([CH2:3][CH3:4])[CH3:2]

Participants

Reactant 2

HCID 12428590HCID 12428590, compound

HCID 20501892HCID 20501892, compound

Product 1

HCID 178449188HCID 178449188, compound

Procedure

By following the procedure of Example 1, but substituting N-sec-butyl-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the desired compound was obtained with a melting point of 133.5°-135.0° C.

Sources & evidence

ORD record: ord-f5f0a26f3c02424799a8a3f784a3b000
Source dataset: uspto-grants-1977_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04057636

Reaction notes

Loading…