Acetic Anhydride → 1-Acetoxy-2-(3-carbethoxypropyl)cyclohex-1-ene

Reaction equation

[C:1]([CH2:6][CH2:7][CH2:8][CH:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C:10]1=[O:15])([O:3][CH2:4][CH3:5])=[O:2].[C:16](OC(=O)C)(=[O:18])[CH3:17]>>[C:16]([O:15][C:10]1[CH2:11][CH2:12][CH2:13][CH2:14][C:9]=1[CH2:8][CH2:7][CH2:6][C:1]([O:3][CH2:4][CH3:5])=[O:2])(=[O:18])[CH3:17]

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 566648HCID 566648, compound

Product 1

HCID 204657141-Acetoxy-2-(3-carbethoxypropyl)cyclohex-1-ene

Procedure

Treatment of 2-(3-carbethoxypropyl)cyclohexane-1-one (Example 14) with acetic anhydride by the procedure of Example 24 is productive of the subject compound.

Sources & evidence

ORD record: ord-85bae14718ca4c808ca41c20da828f08
Source dataset: uspto-grants-1977_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04060540

Reaction notes

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