3-Ethyl-2,4-dimethylnitrobenzene → HCID 21396319, compound

Reaction equation

C(C1C(C)=C([N+]([O-])=O)C=CC=1C)C.[CH2:14]([C:16]1[C:21]([CH3:22])=[CH:20][CH:19]=[C:18]([N+:23]([O-])=O)[C:17]=1[CH2:26][C:27](=O)[C:28]([OH:30])=[O:29])[CH3:15]>>[CH2:14]([C:16]1[C:21]([CH3:22])=[CH:20][CH:19]=[C:18]2[C:17]=1[CH:26]=[C:27]([C:28]([OH:30])=[O:29])[NH:23]2)[CH3:15]

Participants

Reactant 2

HCID 213963293-Ethyl-2,4-dimethylnitrobenzene

HCID 21396338HCID 21396338, compound

Product 1

HCID 21396319HCID 21396319, compound

Procedure

The compound was prepared via 3-ethyl-2,4-dimethylnitrobenzene (b.p. 141°-145° C/11mm Hg) and 3-(2-ethyl-3-methyl-6-nitrophenyl)-pyruvic acid (m.p. 135° C (decomp.).

Sources & evidence

ORD record: ord-b5cfaf50ef054dae990c32db3c6be9bf
Source dataset: uspto-grants-1977_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04060626

Reaction notes

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