3-Bromobenzyl alcohol → N-[3-(3-Bromophenylmethoxy)-5-chloro-2-pyrazinyl]-2,3-dichlorobenzenesulphonamide

HRID 1444012

Reaction equation

HRID 1444012 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH2:5][OH:6].[Cl:10][C:11]1[C:16]([Cl:17])=[CH:15][CH:14]=[CH:13][C:12]=1[S:18]([NH:21][C:22]1[C:27](Cl)=[N:26][C:25]([Cl:29])=[CH:24][N:23]=1)(=[O:20])=[O:19]>>[Br:1][C:2]1[CH:3]=[C:4]([CH2:5][O:6][C:27]2[C:22]([NH:21][S:18]([C:12]3[CH:13]=[CH:14][CH:15]=[C:16]([Cl:17])[C:11]=3[Cl:10])(=[O:20])=[O:19])=[N:23][CH:24]=[C:25]([Cl:29])[N:26]=2)[CH:7]=[CH:8][CH:9]=1

Participants

3

Reactant 2

HCID 851413-Bromobenzyl alcoholHCID 101263402,3-dichloro-N-(3,5-dichloro-2-pyrazinyl)benzenesulphonamide

Product 1

HCID 59168165N-[3-(3-Bromophenylmethoxy)-5-chloro-2-pyrazinyl]-2,3-dichlorobenzenesulphonamide

Procedure

Prepared by the method of Example 31b using 3-bromobenzylalcohol (1.3 g) and 2,3-dichloro-N-(3,5-dichloro-2-pyrazinyl)benzenesulphonamide (Example 74) (1.1 g). Yield is 1.1 g.

Workup

  1. customPrepared by the method of Example 31b

Sources & evidence

ORD record
ord-d2ae341aea184357bb57ed098a387106
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Linked notes

Loading…