4-Methoxy-3-methylbenzoic Acid → HCID 57528000, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=O)=[CH:5][C:4]=1[CH3:12].[C:13]1([CH:19]([NH2:23])[CH2:20][CH2:21][CH3:22])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH:23][CH:19]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH2:20][CH2:21][CH3:22])=[O:9])=[CH:5][C:4]=1[CH3:12]

Participants

Reactant 2

HCID 27595834-Methoxy-3-methylbenzoic Acid

HCID 36037851-Phenylbutan-1-amine

Product 1

HCID 57528000HCID 57528000, compound

Procedure

Prepared in a similar manner to example 4 using 4-methoxy-3-methyl-benzoic acid and 1-phenyl-butylamine. MS (M+H, 298.2).

Sources & evidence

ORD record: ord-fb9875a091cb4032b6ade61d7a9a5316
Source dataset: uspto-grants-2009_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07476399B2

Reaction notes

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