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3-Methoxyphenylhydrazine hydrochloride → [3-(6-Methoxy-2-methyl-1H-indol-3-ylsulfanyl)-phenyl]-acetic acid

HRID 1466757
Notes
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Reaction equation

HRID 1466757 reaction equation
O=[C:2]([CH3:15])[CH2:3][S:4][C:5]1[CH:6]=[C:7]([CH2:11][C:12]([OH:14])=[O:13])[CH:8]=[CH:9][CH:10]=1.Cl.[CH3:17][O:18][C:19]1[CH:20]=[C:21]([NH:25]N)[CH:22]=[CH:23][CH:24]=1>>[CH3:17][O:18][C:19]1[CH:20]=[C:21]2[C:22]([C:3]([S:4][C:5]3[CH:6]=[C:7]([CH2:11][C:12]([OH:14])=[O:13])[CH:8]=[CH:9][CH:10]=3)=[C:2]([CH3:15])[NH:25]2)=[CH:23][CH:24]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 27239403-Methoxyphenylhydrazine hydrochlorideHCID 66765032[3-(2-Oxo-propylsulfanyl)-phenyl]-acetic acid

Product 1

HCID 56840410[3-(6-Methoxy-2-methyl-1H-indol-3-ylsulfanyl)-phenyl]-acetic acid

Procedure

Prepared according to the procedure described in Example 2, Step 1, using the following starting materials: [3-(2-oxo-propylsulfanyl)-phenyl]-acetic acid and 3-methoxyphenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-9489ae006cd64fb4b873029867fc7a1e
Source dataset
uspto-grants-2015_04
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US09000025B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes