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m-Chlorophenylhydrazine hydrochloride → HCID 66765411, compound

HRID 1466847
Notes
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Reaction equation

HRID 1466847 reaction equation
[CH2:1]([O:3][C:4](=[O:20])[C:5]1[CH:10]=[C:9]([S:11][CH2:12][C:13](=O)[CH3:14])[CH:8]=[C:7]([C:16]([F:19])([F:18])[F:17])[CH:6]=1)[CH3:2].Cl.[Cl:22][C:23]1[CH:24]=[C:25]([NH:29]N)[CH:26]=[CH:27][CH:28]=1>>[CH2:1]([O:3][C:4](=[O:20])[C:5]1[CH:6]=[C:7]([C:16]([F:19])([F:18])[F:17])[CH:8]=[C:9]([S:11][C:12]2[C:26]3[C:25](=[CH:24][C:23]([Cl:22])=[CH:28][CH:27]=3)[NH:29][C:13]=2[CH3:14])[CH:10]=1)[CH3:2]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 66764760HCID 66764760, compound

Product 1

HCID 66765411HCID 66765411, compound

Procedure

Prepared according to the procedure described in Example 2, Step 1, using the following starting materials: 3-trifluoromethyl-5-(2-oxo-propylsulfanyl)-benzoic acid ethyl ester and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-fe9126cce72640c384e673db58127ff4
Source dataset
uspto-grants-2015_04
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US09000025B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes