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Sodium borohydride → HCID 65093641, compound

HRID 1476677
Notes
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Reaction equation

HRID 1476677 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][C:6]1[N:10]=[C:9]([C:11](OC)=[O:12])[O:8][N:7]=1.[BH4-].[Na+]>CO>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][C:6]1[N:10]=[C:9]([CH2:11][OH:12])[O:8][N:7]=1
ParticipantsProcedureSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 4311764Sodium borohydrideHCID 67258132HCID 67258132, compound

Product 1

HCID 65093641HCID 65093641, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In analogy to the procedure described for example D26 methyl 3-(3-methoxypropyl)-1,2,4-oxadiazole-5-carboxylate (990 mg) and sodium borohydride (386 mg) in MeOH yield the title compound as an oil.

Sources & evidence

ORD record
ord-0d3ff5202e5444ab80e573d326a27ed0
Source dataset
uspto-grants-2015_04
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US09018175B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes