N,N-diethylpiperidin-4-amine → 1-((E)-2-Decenoyl)-4-diethylaminopiperidine

Reaction equation

[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:13]([N:15]([CH2:22][CH3:23])[CH:16]1[CH2:21][CH2:20][NH:19][CH2:18][CH2:17]1)[CH3:14]>>[C:1]([N:19]1[CH2:20][CH2:21][CH:16]([N:15]([CH2:22][CH3:23])[CH2:13][CH3:14])[CH2:17][CH2:18]1)(=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

Reactant 2

HCID 2758239N,N-diethylpiperidin-4-amine

HCID 5282724trans-2-Decenoic acid

Product 1

HCID 898817921-((E)-2-Decenoyl)-4-diethylaminopiperidine

Procedure

The same procedures as in Example 2 were carried out using (E)-2-decenoic acid and 4-diethylaminopiperidine as starting raw materials, to produce an intended compound.

Workup

customto produce an intended compound

Sources & evidence

ORD record: ord-2618bbe24e9d4225803cb7b13f882ff9
Source dataset: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09428477B2

Reaction notes

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