2-(2,4-Dichlorophenoxy)ethanol → 2-(2,4-Dichlorophenoxy)ethanol sulfamate

HRID 1493991Notes

Reaction equation

HRID 1493991 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:16]=[C:15]([Cl:17])[CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][OH:12]>>[Cl:6][C:7]1[CH:16]=[C:15]([Cl:17])[CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][O:12][S:1](=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 84442-(2,4-Dichlorophenoxy)ethanolHCID 24499Chlorosulfamic acid

Product 1

HCID 191086892-(2,4-Dichlorophenoxy)ethanol sulfamate

Procedure

The title compound was prepared by the procedures of Example 16 from sulfamoyl chloride and 2-(2,4-dichlorophenoxy)ethanol. The viscous oil obtained solidified and was recrystallized from isopropyl ether to give the solid title compound, mp 75°-77° C., in 35% yield.

Workup

  1. customThe viscous oil obtained solidified
  2. customwas recrystallized from isopropyl ether

Sources & evidence

ORD record
ord-f81a0856fbee49febc991eb49bc4419c
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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