HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 6-Tert-butyl-1,3,6-dioxazocan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | tert-Butyldiethanolamine | HCID 62430 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 6-Tert-butyl-1,3,6-dioxazocan-2-one | HCID 118380276 | — |
Reaction Steps
The procedure of Example 1 was followed using N-tert-butyl diethanolamine (16.4 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding a clear oil containing a non-isolable amount of product within a mixture of oligomeric diethanolamines.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09215876B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-bac389f3e44140cb85ac30df467c1168 |
| Source note | uspto-grants-2015_12 |