1,2-Dibromoethane → HCID 67997599, compound

Reaction equation

[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][S:9]([CH3:12])(=[O:11])=[O:10])=[N:6][CH:7]=1.Br[CH2:14][CH2:15]Br>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2([S:9]([CH3:12])(=[O:11])=[O:10])[CH2:15][CH2:14]2)=[N:6][CH:7]=1

Participants

Reactant 2

HCID 78391,2-Dibromoethane

HCID 67997695HCID 67997695, compound

Product 1

HCID 67997599HCID 67997599, compoundYield 19%

Procedure

The title compound was prepared from 5-bromo-2-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 19% of theory; LC (method 3): tR=2.52 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.

Sources & evidence

ORD record: ord-0cd3861758b54c989b8cf38acea4d91a
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09090605B2

Reaction notes

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