Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- → HCID 178457125, compound

HRID 1577551

Reaction equation

HRID 1577551 reaction equation
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C([O-])(=O)C.[CH2:23]([NH3+:26])[CH2:24][CH3:25]>>[CH2:23]([NH:26]/[C:1](/[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)=[C:9]1\[C:10](=[O:18])[C:11]2[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=2[S:13]\1)[CH2:24][CH3:25]

Participants

3

Reactant 2

HCID 4712192Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl-HCID 22348537n-Propylammonium acetate

Product 1

HCID 178457125HCID 178457125, compoundYield 68%

Procedure

Prepared as in Example 35 from 2-benzoyl-benzo[b]thiophen-3-ol and n-propylammonium acetate with a yield of 68% of theory; m.p. 124°-125° C. (petroleum ether/ethyl acetate 1:1).

Sources & evidence

ORD record
ord-afe10ea6926b4ef78a7796c941ba6ff6
Source dataset
uspto-grants-1981_09
Patent number
US04288437

Linked notes

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