Acetohydrazide → HCID 178475140, compound
Reaction equation
[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10](=[NH:14])OCC.[C:15]([NH:18][NH2:19])(=[O:17])[CH3:16]>CO>[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10]([NH:19][NH:18][C:15](=[O:17])[CH3:16])=[NH:14]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In 200 ml. of methanol, 12 g. (0.06 mole) of ethyl 1-methyl-5-nitro-2-imidazolecarboximidate and 4.9 g. (0.066 mole) of acetyl hydrazine are refluxed for 30 hours. The yellow compound is collected, washed with cold methanol and dried to give 12.97 g. of the title compound, melting point 294°C.
Workup
- customThe yellow compound is collected
- washwashed with cold methanol
- customdried
- customto give 12.97 g
Sources & evidence
- ORD record
- ord-6646db82708743fe97c41ba1da41885f
- Source dataset
- uspto-grants-1976_02
- Patent number
- US03940411
Reaction notes
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