Methanesulfonyl chloride → 2-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

HRID 15873

Reaction equation

HRID 15873 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[CH2:5][CH2:6][OH:7].[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:7][CH2:6][CH2:5][C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([NH:1][S:12]([CH3:11])(=[O:14])=[O:13])[CH:3]=1)(=[O:14])=[O:13]

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 149389872-(3-Aminophenyl)ethan-1-ol

Product 1

HCID 574443592-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

Procedure

The title compound was prepared from 3-aminophenethyl alcohol (U.S. Pat. No. 2,641,602) and methanesulfonyl chloride (2 eq.) according to the procedure contained within description 4. The product was used immediately without further purification or characterisation.

Workup

  1. customThe product was used immediately without further purification or characterisation

Sources & evidence

ORD record
ord-df39bbbc55b94cc4a4671516af5755d6
Source dataset
uspto-grants-2010_06
Patent number
US07732600B2

Linked notes

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