Reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]([NH:17][C:18](=[O:28])[CH:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH2:20][CH3:21])[CH2:11][C:12]([O:14][CH2:15][CH3:16])=[O:13])[CH:7]=[CH:8][CH:9]=1)([O-])=O.[Sn](Cl)Cl>>[NH2:1][C:4]1[CH:5]=[C:6]([CH:10]([NH:17][C:18](=[O:28])[CH:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH2:20][CH3:21])[CH2:11][C:12]([O:14][CH2:15][CH3:16])=[O:13])[CH:7]=[CH:8][CH:9]=1Participants
3
Procedure
Corresponding to Example 3b, 6.3 g of (7a) were reduced using tin-(II) dichloride. A white solid was obtained (yield: 3.9 g).
Workup
- customA white solid was obtained (yield: 3.9 g)
Sources & evidence
- ORD record
- ord-b68cc9f9bdc64f529ceefc78ccb467ef
- Source dataset
- uspto-grants-2001_09
- Patent number
- US06291503B1
Linked notes
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