HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furfural diethyl acetal → 2-(Diethoxymethyl)-5-(tributylstannyl) furan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furfural diethyl acetal | HCID 83553 | — |
| Reactant | 2-(Diethoxymethyl)-5-(tributylstannyl) thiophene | HCID 15434854 | — |
| Product | 2-(Diethoxymethyl)-5-(tributylstannyl) furan | HCID 15434861 | 82% |
Reaction Steps
Following the procedure for preparing 2-(diethoxymethyl)-5-(tributylstannyl)-thiophene as described in step (1) of Example 1, 17 g (10 mmol) of 2-(diethoxymethyl)furan was converted to 32.6 g (82% yield) of 2-(diethoxymethyl)-5-(tributylstannyl) furan (bp 110° C., 1 torr).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05994394 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-05e3189ee62643b59d248db4b713fd4b |
| Source note | uspto-grants-1999_11 |