Bromine → 2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine
Reaction equation
[NH2:1][C:2]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:3]=1[CH2:4][N:5]([CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1)[CH2:6][CH3:7].[Br:20]Br>C(Cl)Cl>[NH2:1][C:2]1[C:17]([Br:20])=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:3]=1[CH2:4][N:5]([CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1)[CH2:6][CH3:7]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine was prepared from 2-amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine and bromine analogous to Example 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride):
Sources & evidence
- ORD record
- ord-cdda6805ab864a4cb313a3552dba3bf1
- Source dataset
- uspto-grants-1976_04
- Patent number
- US03950393
Reaction notes
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