Ethanolamine → 2-Hydroxyethyl Methacrylate

HRID 1608751

Reaction equation

HRID 1608751 reaction equation
[C:1]([OH:6])(=[O:5])[C:2]([CH3:4])=[CH2:3].C1(N=C=NC2CCCCC2)CCCCC1.[CH2:22]([CH2:24][NH2:25])[OH:23]>>[C:1]([NH:25][CH2:24][CH2:22][OH:23])(=[O:6])[C:2]([CH3:4])=[CH2:3].[C:1]([O:6][CH2:24][CH2:22][OH:23])(=[O:5])[C:2]([CH3:4])=[CH2:3]

Participants

5

Procedure

2-methacrylamidoethyl alcohol was prepared in substantially the same manner as in Example 11 except that 6.9 g of methacrylic acid and 16.5 g of dicyclohexylcarbodiimide and 4.9 g of ethanolamine were used. Subsequently, a polymer powder was obtained in substantially the same manner as in Example 11 except that 52.0 g of 2-methacryloyloxyethyl alcohol was used. The obtained polymer powder is referred to as "1T-40". Separately, 2-methacrylamidoethyl alcohol was prepared in substantially the same manner as in Example 11 except that 27.6 g of methacrylic acid and 66.0 g of dicyclohexylcarbodiimide and 19.6 g of ethanolamine were used. Subsequently, a polymer powder was obtained in substantially the same manner as in Example 11 except that 20.8 g of 2-methacryloyloxyethyl alcohol was used. The polymer powder is referred to as "4T-40".

Sources & evidence

ORD record
ord-78df785917ab4fe5ba0754ab1b7d4924
Source dataset
uspto-grants-1995_03
Patent number
US05397682

Linked notes

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