Chlorosulfamic acid → HCID 19108682, compound

Reaction equation

[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][OH:15])=[CH:10][CH:9]=1>>[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][O:15][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:10][CH:9]=1

Participants

Reactant 2

HCID 24499Chlorosulfamic acid

HCID 2200792-(4-Methoxyphenoxy)ethanol

Product 1

HCID 19108682HCID 19108682, compoundYield 54%

Procedure

The title compound was prepared by procedures of Example 28 from sulfamoyl chloride and 2-(4-methoxyphenoxy)ethanol in 54% yield as an off-white solid, mp 84°-87° C.

Sources & evidence

ORD record: ord-472a46ea4e884d79b6fead87928decc0
Source dataset: uspto-grants-1993_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05192785

Reaction notes

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