4-Bromo-2-methylpyridine → HCID 67015516, compound
Reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[CH3:22])[CH2:9][C:10](N(OC)C)=[O:11])[CH:5]=[CH:6][CH:7]=1.Br[C:24]1[CH:29]=[CH:28][N:27]=[C:26]([CH3:30])[CH:25]=1>>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[CH3:22])[CH2:9][C:10]([C:24]2[CH:29]=[CH:28][N:27]=[C:26]([CH3:30])[CH:25]=2)=[O:11])[CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
In analogy to example 74, step 5, from 3-(3-bromo-phenyl)-N-methoxy-N-methyl-3-o tolyl-propionamide and 4-bromo-2-methylpyridine was prepared the title compound as a colorless oil, MS (ESI+): m/z=394.08 ([M+H]+, 1 Br).
Sources & evidence
- ORD record
- ord-4b75d24fda2a4bfbb28916bfd186773f
- Source dataset
- uspto-grants-2014_07
- Patent number
- US08765730B2