Water → 5-Phenyl-2,4-pentadienoic acid

Reaction equation

S([O-])([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C)(=O)=O.[OH2:18]>>[CH:8]([CH:7]=[CH:6][C:5]([OH:4])=[O:18])=[CH:9][C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

Reactant 2

HCID 962Water

HCID 4329331Npc315034

Product 1

HCID 737775-Phenyl-2,4-pentadienoic acid

Conditions

Temperature: 80 °C

Procedure

A 2 l reactor with stirrer and reflux condenser was charged with 433 g of deionized water, and 3 grams of lauryl sulfate (30% strength solution), this initial charge then being heated to 80° C. with stirring under a nitrogen atmosphere.

Workup

temperatureA 2 l reactor with stirrer and reflux condenser
additionthis initial charge

Sources & evidence

ORD record: ord-ca771bd158b447c2b3b0adaced31c75c
Source dataset: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08784606B2

Reaction notes

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