HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N-(3-Methoxybenzylidene)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-(3-Methoxybenzylidene)aniline | HCID 555084 | — |
Reaction Steps
A solution of 85.4 gm. of 3-methoxybenzaldehyde, 58.7 gm. of aniline, and 185 gm. of 3A molecular sieves in 700 ml. of anhydrous ether was refluxed for 16 hours. The ether was dried (Na2SO4), filtered, and concentrated in vacuo to an oil which upon distillation provided 93.2 gm of oil. b.p. 141°-143°/0.5 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04476311 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-312d2c2fdff149489cd828aa97a97e7e |
| Source note | uspto-grants-1984_10 |