HCID 23050238, compound → HCID 178486609, compound

Reaction equation

COC1C(OC)=CC2SC(/C=C/C#N)=CC=2C=1.[ClH:18].[OH:19][NH:20][C:21](=[NH:37])/[CH:22]=[CH:23]/[C:24]1[S:28][C:27]2[CH:29]=[C:30]([O:35][CH3:36])[C:31]([O:33][CH3:34])=[CH:32][C:26]=2[CH:25]=1>>[ClH:18].[OH:19][NH:20][C:21](=[NH:37])[CH:22]=[CH:23][C:24]1[S:28][C:27]2[CH:29]=[C:30]([O:35][CH3:36])[C:31]([O:33][CH3:34])=[CH:32][C:26]=2[CH:25]=1

Participants

Reactant 2

HCID 23050238HCID 23050238, compound

HCID 178486608HCID 178486608, compound

Product 1

HCID 178486609HCID 178486609, compound

Procedure

Using the procedure described in Example 2 (E)-3-(5,6-dimethoxy-benzo[b]thiophene-2-yl)-2-propenenitrile was converted into (E)-N-hydroxy-3-(5,6-dimethoxy-benzo[b]thiophene-2-yl)-prop-2-eneimidamide hydrochloride, m.p. 188°-198° C. (decomp.).

Sources & evidence

ORD record: ord-f9cff82d38184125959c0e210f1a69b8
Source dataset: uspto-grants-1990_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04929636

Reaction notes

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