Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dicyclopentadiene | HCID 6492 | — |
| Reactant | (2R,3S,4S,5R,6R)-2-(hydroxymethyl)-6-[(E)-3-phenylprop-2-enoxy]oxane-3,4,5-triol | HCID 5280656 | — |
| Product | Rosin Dicyclopentadiene | HCID 131718860 | — |
Reaction Steps
Proportions of phenolic-modified rosin (from Example 1) and dicyclopentadiene, as indicated in Table II, were charged into a one-liter autoclave reactor. The charged autoclave was purged with nitrogen and sealed. The reaction mixture was heated to 260° C. within 60 minutes and maintained at 260° C. for six hours. The reactor then was vented carefully, and the molten resin poured into an aluminum pan and allowed to cool.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05403391 |
|---|
| Source dataset | uspto-grants-1995_04 |
|---|
| ORD ID | ord-1e1c3b7e571045d1992897fdf2e1e6be |
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| Source note | uspto-grants-1995_04 |
|---|
