2-Mercaptoethanol → Dibutyl-zinn [German]

HRID 1657128

Reaction equation

HRID 1657128 reaction equation
[CH2:1]([Sn:5](=O)[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].SCCO>C1(C)C=CC=CC=1>[CH2:1]([Sn:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 15672-MercaptoethanolHCID 61221Dibutyltin oxide

Product 1

HCID 6484Dibutyl-zinn [German]Yield 154.5%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Following the procedure of Example 1, 24.9 g (0.10 mole) dibutyltin oxide was reacted with 15.6 g (0.20 mole) 2-mercaptoethanol in toluene to give 36 g of dibutyltin-bis-(2-hydroxyethylmercaptide), a light yellow liquid.

Sources & evidence

ORD record
ord-62d2f22050524ae189b28b5eec3fb25e
Source dataset
uspto-grants-1993_10
Patent number
US05256704

Linked notes

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