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5-Methylfuran-2-carbonyl chloride → HCID 21530238, compound

HRID 1657777
Notes
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Reaction equation

HRID 1657777 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][NH:13][CH:12]([CH3:16])[CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:17][C:18]1[O:22][C:21]([C:23]([Cl:25])=[O:24])=[CH:20][CH:19]=1>C1C=CC=CC=1>[ClH:25].[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][N:13]([C:23]([C:21]3[O:22][C:18]([CH3:17])=[CH:19][CH:20]=3)=[O:24])[CH:12]([CH3:16])[CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 27598515-Methylfuran-2-carbonyl chlorideHCID 215302811-(3-Phenylpropyl)-3-methylpiperazine

Product 1

HCID 21530238HCID 21530238, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of 1-(3-phenylpropyl)-3-methylpiperazine, 5-methyl-2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-ad61e29d5eae4351989cee8209ea7d21
Source dataset
uspto-grants-1976_06
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US03962249

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes