Acrylamide → HCID 86738175, compound
Reaction equation
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH2:18][CH:19]=[CH2:20])[CH:10]=[CH:11][CH:12]=[C:13]([C:16]#[N:17])[C:14]#[N:15])[CH:7]=[CH2:8]>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH:10]=[CH:11][CH:12]=[C:13]([C:14]#[N:15])[C:16]#[N:17])[CH2:18][CH:19]=[CH2:20])[CH:7]=[CH2:8]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 40 g. of acrylamide, 52 g. of 3-diallylaminoallylidenemalononitrile (A) in 900 cc. of ethanol was refluxed. 1.3 g. of AZBN was added and the solution refluxed for two hours. At two hour time intervals, the following solutions were added in this order by refluxing:
Workup
- additionof AZBN was added
- temperaturethe solution refluxed for two hours
- additionthe following solutions were added in this order
- temperatureby refluxing
Sources & evidence
- ORD record
- ord-a20e085380b54c7fbce2344106db85a8
- Source dataset
- uspto-grants-1981_12
- Patent number
- US04307184
Reaction notes
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