2-Amino-1-naphthalenol → HCID 22764064, compound
Reaction equation
[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]=1[OH:12].[Cl:13][CH2:14][C:15](OCC)(OCC)OCC>C(O)C>[Cl:13][CH2:14][C:15]1[O:12][C:3]2[C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[CH:10]=[CH:11][C:2]=2[N:1]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Prepared by reacting 2.93 g of 2-amino-1-naphthol with 3.54 g of 2-chloro-1,1,1-triethoxy-ethane in 25 ml of ethanol at 60° C.
Workup
- customPrepared
- customat 60° C.
Sources & evidence
- ORD record
- ord-51d8fa68c590407da9b9b23345e27736
- Source dataset
- uspto-grants-2011_10
- Patent number
- US08034941B2
Reaction notes
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