7-Bromooct-1-ene → n-Methyloct-5-en-1-amine tosylate salt
Reaction equation
Br[CH:2]([CH3:9])[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].[S:10]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)([OH:13])(=[O:12])=[O:11].[CH3:21][NH:22]CCCCC=C>>[S:10]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)([OH:13])(=[O:12])=[O:11].[CH3:21][NH:22][CH2:9][CH2:2][CH2:3][CH2:4][CH:5]=[CH:6][CH2:7][CH3:8]Participants
3
Procedure
Compound 32c was synthesized from 7-bromo-octene as a white powder in quantitative yield, following the procedure as described for compound 32a.
Sources & evidence
- ORD record
- ord-7141ef725b3a4e4eaa2d18ddfedb800a
- Source dataset
- uspto-grants-2011_08
- Patent number
- US08003659B2
Reaction notes
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