(+-)-4-Methylhexanoic acid → HCID 12600624, compound

Reaction equation

[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5](O)=[O:6].S(Cl)([Cl:12])=O>>[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5]([Cl:12])=[O:6]

Participants

Reactant 2

HCID 15271(+-)-4-Methylhexanoic acid

HCID 24386Thionyl Chloride

Product 1

HCID 12600624HCID 12600624, compound

Procedure

The acid from step A2 is converted into the acid chloride by interaction with thionyl chloride according to a standard method. After removal of the excess of thionyl chloride, the residual acid chloride is used in step C2 without further purification.

Workup

customAfter removal of the excess of thionyl chloride
customthe residual acid chloride is used in step C2 without further purification

Sources & evidence

ORD record: ord-677e682bdd7c48c3b1e43681e0ff2d2d
Source dataset: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04077260

Reaction notes

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