Acrolein → 4-Methyl-2-vinyl-1,3-dioxane

HRID 1679104

Reaction equation

HRID 1679104 reaction equation
[CH:1]([CH:3]=[CH2:4])=[O:2].[CH2:5](O)[CH2:6][CH:7]([OH:9])[CH3:8]>>[CH:3]([CH:1]1[O:9][CH:7]([CH3:8])[CH2:6][CH2:5][O:2]1)=[CH2:4]

Participants

3

Reactant 2

HCID 7847AcroleinHCID 78961,3-Butanediol

Product 1

HCID 1108964-Methyl-2-vinyl-1,3-dioxaneYield 99%

Procedure

When acrolein is condensed with 1,3-butanediol, the product obtained is 2-vinyl-4-methyl-1,3-dioxane (99 percent yield).

Workup

  1. customthe product obtained

Sources & evidence

ORD record
ord-28c4dee2e46945d589c1baefb898e4ed
Source dataset
uspto-grants-1978_03
Patent number
US04079064

Linked notes

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