Dibutylamine → HCID 23454947, compound
Reaction equation
C(NCCCC)CCC.C(NNC1C=CC(N=C=S)=CC=1)=O.[CH:23]([NH:25][NH:26][C:27]1[CH:32]=[CH:31][C:30]([NH:33][C:34]([N:36]([CH2:44][C:45]2C=CC=[CH:47][CH:46]=2)[CH2:37][C:38]2C=CC=[CH:40][CH:39]=2)=[S:35])=[CH:29][CH:28]=1)=[O:24]>>[CH:23]([NH:25][NH:26][C:27]1[CH:28]=[CH:29][C:30]([NH:33][C:34]([N:36]([CH2:44][CH2:45][CH2:46][CH3:47])[CH2:37][CH2:38][CH2:39][CH3:40])=[S:35])=[CH:31][CH:32]=1)=[O:24]Participants
4
Procedure
Di-n-butylamine (0.13 g, 0.001 mole) and 4-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.10 g (31 percent), m.p. 139°-141° C.
Sources & evidence
- ORD record
- ord-d0e69342806549b487cbcafa57ff9d45
- Source dataset
- uspto-grants-1981_06