3-Pyrroline → HCID 23454968, compound

Reaction equation

N1CC=CC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:19]([NH:21][NH:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29][C:30]([N:32]([CH2:40][C:41]2[CH:46]=[CH:45]C=CC=2)CC2C=CC=CC=2)=[S:31])=[CH:25][CH:24]=1)=[O:20]>>[CH:19]([NH:21][NH:22][C:23]1[CH:24]=[CH:25][C:26]([NH:29][C:30]([N:32]2[CH2:40][CH:41]=[CH:46][CH2:45]2)=[S:31])=[CH:27][CH:28]=1)=[O:20]

Participants

Reactant 3

HCID 660593-Pyrroline

HCID 23454956HCID 23454956, compound

HCID 23454969HCID 23454969, compound

Product 1

HCID 23454968HCID 23454968, compound

Procedure

3-Pyrroline (0.069 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.18 g (69 percent), m.p. 218°-220° C.

Sources & evidence

ORD record: ord-9547ce2a39e745c9a2f9fc6fc3108cdf
Source dataset: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04276364

Reaction notes

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