Phosgene → HCID 59377726, compound

Reaction equation

[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][C:6]=1[O:12][CH3:13])(=[O:4])=[O:3].[C:14](Cl)(Cl)=[O:15]>>[N:11]([C:8]1[CH:9]=[CH:10][C:5]([S:2]([CH3:1])(=[O:3])=[O:4])=[C:6]([O:12][CH3:13])[CH:7]=1)=[C:14]=[O:15]

Participants

Reactant 2

HCID 6371Phosgene

HCID 223167444-Methanesulfonyl-3-methoxyaniline

Product 1

HCID 59377726HCID 59377726, compound

Procedure

4-Isocyanato-1-methanesulfonyl-2-methoxy-benzene was prepared by reaction of 4-methanesulfonyl-3-methoxy-phenylamine with phosgene following the procedure of step 6 of Example 3.

Sources & evidence

ORD record: ord-b744636075954b54a421e10e84e723af
Source dataset: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08153809B2

Reaction notes

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