Silane, dimethoxybis(1-methylethyl)- → HCID 53833435, compound

Reaction equation

[CH:1]([Si:4]([CH:7]([CH3:9])[CH3:8])(Cl)[Cl:5])([CH3:3])[CH3:2].C([Si](C(C)C)(OC)[O:14][CH3:15])(C)C>>[CH:1]([Si:4]([CH:7]([CH3:9])[CH3:8])([O:14][CH3:15])[Cl:5])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 87520Silane, dimethoxybis(1-methylethyl)-

HCID 2758384Diisopropyldichlorosilane

Product 1

HCID 53833435HCID 53833435, compound

Procedure

A 500 ml-capacity, four-necked flask was charged with 18.5 g (0.1 moles) of diisopropyldichlorosilane and 17.6 g (0.1 moles) of diisopropyldimethoxysilane, and the resulting mixture was stirred at 20° C.-30° C. for 1 hour. There occurred a disproportionation reaction, thus giving a mixture comprising diisopropylmethoxychlorosilane, the unreacted diisopropyldichlorosilane and the unreacted diisopropyldimethoxysilane.

Workup

customa disproportionation reaction

Sources & evidence

ORD record: ord-c145beb8a87f4d5682ec80ea2032b8fc
Source dataset: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08163950B2

Reaction notes

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