HCID 45273676, compound → HCID 59831679, compound
Reaction equation
CO[C:3](=O)[NH:4][CH2:5][CH2:6][CH:7]([C:14]1[CH:22]=[C:21]2[C:17]([CH:18]=[CH:19][NH:20]2)=[CH:16][CH:15]=1)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.N1C2C(=CC(C(C3C=CC=CC=3)CCNC)=CC=2)C=C1>>[NH:20]1[C:21]2[C:17](=[CH:16][CH:15]=[C:14]([CH:7]([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)[CH2:6][CH2:5][NH:4][CH3:3])[CH:22]=2)[CH:18]=[CH:19]1Participants
3
Procedure
[3-(1H-Indol-6-yl)-3-phenyl-propyl]-methyl-amine (110 mg, 24% yield) XVI was prepared as a hydrochloride salt from [3-(1H-indol-6-yl)-3-phenyl-propyl]-carbamic acid methylester (XV), using the procedure described for preparation of [3-(1H-indol-5-yl)-3-phenyl-propyl]-methyl-amine XI (see Example 2). MS (M+H)=265.
Sources & evidence
- ORD record
- ord-0e5a049a06a74fc797930791e4b63f62
- Source dataset
- uspto-grants-2010_09